Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tert-butyl malonate → HCID 178516617, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tert-butyl malonate | HCID 21883978 | — |
| 반응물 | Sodium t-butoxide | HCID 23676156 | — |
| 반응물 | 1-Isocyano-2-methylpropan-2-yl methyl carbonate | HCID 25267464 | — |
| 반응물 | 4-(4,4-Difluorocyclohexyl)benzaldehyde | HCID 57488488 | — |
| 반응물 | HCID 178507353 | HCID 178507353 | — |
| 생성물 | HCID 178516617 | HCID 178516617 | — |
반응 단계
The compound was synthesized starting from 1H-benzo[d]imidazol-5-amine (0.71 g, 5.35 mmol), 4-(4,4-difluorocyclohexyl)benzaldehyde (1.2 g, 5.35 mmol), mono-tert-butyl malonate (0.850 mg, 5.35 mmol), 1-isocyano-2-methylpropan-2-yl methyl carbonate (0.84 g, 5.35 mmol) and sodium tert.-butoxide (0.615 g, 5.5 mmol) according to method 5.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08530670B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-d5bd49c8629944f98017c1268e0c9400 |
| 출처 메모 | uspto-grants-2013_09 |