참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 2-(2-Bromoethyl)naphthalene | HCID 228270 | — |
| 생성물 | 2-(2-Bromoethyl)naphthalenesulfonic acid | HCID 86612694 | — |
반응 단계
2-(2-bromoethyl)naphthalene (120 g) was stirred in an ice bath while fuming sulfuric acid (50 g) was slowly added dropwise. After the dropwise addition, the mixture was stirred at 0° C. for 30 hours, whereby 2-(2-bromoethyl)naphthalenesulfonic acid and a plurality of isomers were obtained, and then separated and purified.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08093342B2 |
|---|
| 출처 데이터셋 | uspto-grants-2012_01 |
|---|
| ORD ID | ord-ebce4216be1f4dd7b193824955a78eba |
|---|
| 출처 메모 | uspto-grants-2012_01 |
|---|
