Ethyl 4-isopropylthiazole-2-carboxylate → 4-Cyclobutylthiazole-2-carboxylic acid ethyl ester
반응식
[C:1](OCC)(=S)C(N)=O.[CH:9]([C:12]1[N:13]=[C:14]([C:17]([O:19][CH2:20][CH3:21])=[O:18])[S:15][CH:16]=1)([CH3:11])[CH3:10]>>[CH2:20]([O:19][C:17]([C:14]1[S:15][CH:16]=[C:12]([CH:9]2[CH2:11][CH2:1][CH2:10]2)[N:13]=1)=[O:18])[CH3:21]참가 물질
3
실험 절차
Compound V2 (yellow oil) was synthesized from compound U2 (23.87 g, 1 eq.) and ethyl thiooxamate (21.41 g, 1 eq.) in 64% yield, following the procedure as described for compound 36.
출처 및 근거
- ORD 기록
- ord-587076b139b0417592189237a82e22d7
- 출처 데이터셋
- uspto-grants-2012_01
- 특허 번호
- US08093379B2
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