3-Chlorothiophenol → 6-benzenesulfonyl-3,4-dihydro-2H-naphthalen-1-one

HRID 420180노트

반응식

HRID 420180 반응식
ClC1C=C(S)C=CC=1.Cl[C:10]1[CH:11]=[C:12]([S:16]([C:19]2[CH:20]=[C:21]3[C:26](=[CH:27][CH:28]=2)[C:25](=[O:29])[CH2:24][CH2:23][CH2:22]3)(=[O:18])=[O:17])[CH:13]=[CH:14][CH:15]=1>>[C:12]1([S:16]([C:19]2[CH:20]=[C:21]3[C:26](=[CH:27][CH:28]=2)[C:25](=[O:29])[CH2:24][CH2:23][CH2:22]3)(=[O:18])=[O:17])[CH:11]=[CH:10][CH:15]=[CH:14][CH:13]=1

참가 물질

3

반응물 2

HCID 162573-ChlorothiophenolHCID 666511846-(3-chloro-benzenesulfonyl)-3,4-dihydro-2H-naphthalen-1-one

생성물 1

HCID 590217396-benzenesulfonyl-3,4-dihydro-2H-naphthalen-1-one

실험 절차

Similarly prepared using the above procedure with 3-chlorobenzenethiol in step 4, was 6-(3-chloro-benzenesulfonyl)-3,4-dihydro-2H-naphthalen-1-one. MS: 287 (M+H)+.

후처리

  1. customSimilarly prepared

출처 및 근거

ORD 기록
ord-020ea02c12904f24b7cf5ded56f361c6
출처 데이터셋
uspto-grants-2012_01
특허 번호
US08093424B2

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