Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Anhydride → N-(4-amino-2-chloropyridin-3-yl)acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | 2-Chloropyridine-3,4-diamine | HCID 285736 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | N-(4-amino-2-chloropyridin-3-yl)acetamide | HCID 45119288 | — |
반응 단계
1.1 A solution of 10.0 g of 3,4-diamino-2-chloropyridine and 6.62 ml of acetic anhydride in 100 ml of THF is stirred at room temperature for 16 hours. The product is separated off and dried, giving 7.3 g of N-(4-amino-2-chloropyridin-3-yl)acetamide (“1”).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08097727B2 |
| 출처 데이터셋 | uspto-grants-2012_01 |
| ORD ID | ord-855e4986caed43f8929211014d5c50e5 |
| 출처 메모 | uspto-grants-2012_01 |