5-Methylsalicylic acid → HCID 11210681, 화합물

HRID 421043

반응식

HRID 421043 반응식
[CH3:1][C:2]1[CH:10]=[C:6]([C:7]([OH:9])=O)[C:5]([OH:11])=[CH:4][CH:3]=1.[F:12][C:13]([F:26])([F:25])[C:14]1[CH:15]=[C:16]([CH:18]=[C:19]([C:21]([F:24])([F:23])[F:22])[CH:20]=1)[NH2:17]>>[F:12][C:13]([F:25])([F:26])[C:14]1[CH:15]=[C:16]([NH:17][C:7](=[O:9])[C:6]2[CH:10]=[C:2]([CH3:1])[CH:3]=[CH:4][C:5]=2[OH:11])[CH:18]=[C:19]([C:21]([F:22])([F:24])[F:23])[CH:20]=1

참가 물질

3

반응물 2

HCID 69735-Methylsalicylic acidHCID 9480Benzenamine, 3,5-bis(trifluoromethyl)-

생성물 1

HCID 11210681HCID 11210681, 화합물수율 54.9%

실험 절차

Using 5-methylsalicylic acid and 3,5-bis(trifluoromethyl)aniline as the raw materials, the same operation as the example 16 gave the title compound.

출처 및 근거

ORD 기록
ord-033ede6e1d0244b0898e507bf63fc497
출처 데이터셋
uspto-grants-2012_01
특허 번호
US08097759B2

연결된 노트

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