5-Bromosalicylic acid → Imd-0560

HRID 421090

반응식

HRID 421090 반응식
[Br:1][C:2]1[CH:10]=[C:6]([C:7]([OH:9])=O)[C:5]([OH:11])=[CH:4][CH:3]=1.[F:12][C:13]([F:26])([F:25])[C:14]1[CH:20]=[CH:19][C:18]([C:21]([F:24])([F:23])[F:22])=[CH:17][C:15]=1[NH2:16]>>[F:12][C:13]([F:25])([F:26])[C:14]1[CH:20]=[CH:19][C:18]([C:21]([F:23])([F:24])[F:22])=[CH:17][C:15]=1[NH:16][C:7](=[O:9])[C:6]1[CH:10]=[C:2]([Br:1])[CH:3]=[CH:4][C:5]=1[OH:11]

참가 물질

3

반응물 2

HCID 69725-Bromosalicylic acidHCID 7198182,5-Bis(trifluoromethyl)aniline

생성물 1

HCID 11464503Imd-0560수율 24%

실험 절차

Using 5-bromosalicylic acid and 2,5-bis(trifluoromethyl)aniline as the raw materials, the same operation as the example 16 gave the title compound.

출처 및 근거

ORD 기록
ord-39d8b89b4fdf4e889136b5c0573a4058
출처 데이터셋
uspto-grants-2012_01
특허 번호
US08097759B2

연결된 노트

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