5-Nitrosalicylic acid → N-[2-Chloro-5-(trifluoromethyl)phenyl]-2-hydroxy-5-nitrobenzamide

HRID 421115

반응식

HRID 421115 반응식
[N+:1]([C:4]1[CH:12]=[C:8]([C:9]([OH:11])=O)[C:7]([OH:13])=[CH:6][CH:5]=1)([O-:3])=[O:2].[Cl:14][C:15]1[CH:21]=[CH:20][C:19]([C:22]([F:25])([F:24])[F:23])=[CH:18][C:16]=1[NH2:17]>>[Cl:14][C:15]1[CH:21]=[CH:20][C:19]([C:22]([F:24])([F:25])[F:23])=[CH:18][C:16]=1[NH:17][C:9](=[O:11])[C:8]1[CH:12]=[C:4]([N+:1]([O-:3])=[O:2])[CH:5]=[CH:6][C:7]=1[OH:13]

참가 물질

3

반응물 2

HCID 73185-Nitrosalicylic acidHCID 8475Benzenamine, 2-chloro-5-(trifluoromethyl)-

생성물 1

HCID 17860170N-[2-Chloro-5-(trifluoromethyl)phenyl]-2-hydroxy-5-nitrobenzamide수율 31.1%

실험 절차

Using 5-nitrosalicylic acid and 2-chloro-5-(trifluoromethyl)aniline as the raw materials, the same operation as the example 16 gave the title compound.

출처 및 근거

ORD 기록
ord-8641323d9ec9481c9a077632017d2ccc
출처 데이터셋
uspto-grants-2012_01
특허 번호
US08097759B2

연결된 노트

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