Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Chloro-5-nitroaniline → 3-chloro-N-(2-chloro-5-nitrophenyl)benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Chloro-5-nitroaniline | HCID 22691 | — |
| 반응물 | Benzoyl chloride, 3-chloro- | HCID 69252 | — |
| 생성물 | 3-chloro-N-(2-chloro-5-nitrophenyl)benzamide | HCID 871095 | — |
반응 단계
2-chloro-5-nitroaniline (Aldrich, 25.7 mmol) was used in general procedure 1 with 3-chlorobenzoyl chloride (26.5 mmol). The product was purified by silica gel chromatography (40% EtOAc/Hex) to give 3-chloro-N-(2-chloro-5-nitrophenyl)benzamide as a brown solid. MS (Q1) 294.0 (M)+
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08101610B2 |
| 출처 데이터셋 | uspto-grants-2012_01 |
| ORD ID | ord-9144608349354df5b1026a8265d1d3cb |
| 출처 메모 | uspto-grants-2012_01 |