Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 423023생성일: 2026년 10월 26일
4-Chlorophenyl cyclopropyl ketone → (4-chlorophenyl)(cyclopropyl)methanone O-methyl oxime
https://huagongshe.com/reaction/423023
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 4-Chlorophenyl cyclopropyl ketone | HCID 81148 | — |
| 반응물 | O-Methylhydroxylamine hydrochloride | HCID 521874 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | (4-chlorophenyl)(cyclopropyl)methanone O-methyl oxime | HCID 73696106 | 87.4% |
반응 단계
Methoxylamine hydrochloride (2.004 g) was added to (4-chlorophenyl)(cyclopropyl)methanone (2.71 g) in pyridine (60 mL) at 25° C. The resulting solution was stirred at 25° C. for 24 hours. The pyridine was removed in vacuo, and the residual solid extracted with ether. Filtration and evaporation of the solvent gave the crude (4-chlorophenyl)(cyclopropyl)methanone O-methyl oxime (2.75 g, 87%) as a yellow oil. This material was used directly in the next step without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US08101623B2 |
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| 출처 데이터셋 | uspto-grants-2012_01 |
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| ORD ID | ord-820c7f43ceda4a6a8685cd0aafeb45e2 |
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| 출처 메모 | uspto-grants-2012_01 |
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