Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylformamide → N'-(6-oxo-7-phenyl-5,6-dihydro-1,5-naphthyridin-2-yl)propanohydrazide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylformamide | HCID 6228 | — |
| 반응물 | Diisopropylethylamine | HCID 81531 | — |
| 반응물 | 6-Hydrazinyl-3-phenyl-1,5-naphthyridin-2(1H)-one | HCID 67069008 | — |
| 생성물 | N'-(6-oxo-7-phenyl-5,6-dihydro-1,5-naphthyridin-2-yl)propanohydrazide | HCID 67094058 | — |
반응 단계
To a mixture of 6-hydrazino-3-phenyl-1,5-naphthyridin-2(1H)-one (7-2) (70 mg, 0.277 mmol) and DIPEA (0.2 mL, 1.15 mmol) in DMF (3 mL) was stirred at room temperature for 0.5 hours. The solvent was removed under reduced pressure to give N′-(6-oxo-7-phenyl-5,6-dihydro-1,5-naphthyridin-2-yl)propanohydrazide (7-3) as yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08536193B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-c3a78af3655f4404a3368cd7f41557c9 |
| 출처 메모 | uspto-grants-2013_09 |