참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Dimethylformamide | HCID 6228 | — |
| 반응물 | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| 반응물 | 1-Fluoro-5-methyl-2,4-dinitrobenzene | HCID 520705 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | [2-(5-Fluoro-2,4-dinitro-phenyl)-vinyl]-dimethyl-amine | HCID 57060726 | 63% |
반응 단계
A mixture of 1-fluoro-5-methyl-2,4-dinitro-benzene (10 g, 50 mmol), dimethoxymethyl-dimethylamine (11.9 g, 100 mmol) and DMF (50 mL) was heated at 100° C. for 4 h. The solution was cooled and poured into water. The red precipitate was collected via filtration, washed with water adequately and dried to give [2-(5-fluoro-2,4-dinitro-phenyl)-vinyl]-dimethyl-amine (8 g, 63%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08101767B2 |
|---|
| 출처 데이터셋 | uspto-grants-2012_01 |
|---|
| ORD ID | ord-58383551095046d48a529bb093c4cd24 |
|---|
| 출처 메모 | uspto-grants-2012_01 |
|---|
