Ethanolamine → HCID 53673871, 화합물

HRID 4240노트

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HRID 4240 반응식
[Br:1][C:2]1[CH:8]=[C:7]([N+:9]([O-:11])=[O:10])[C:6](Br)=[CH:5][C:3]=1[NH2:4].[CH2:13]([CH2:15][NH2:16])[OH:14]>C(O)C>[OH:14][CH2:13][CH2:15][NH:16][C:6]1[CH:5]=[C:3]([NH2:4])[C:2]([Br:1])=[CH:8][C:7]=1[N+:9]([O-:11])=[O:10]

참가 물질

4

반응물 2

HCID 700EthanolamineHCID 111506072,5-Dibromo-4-nitroaniline2회

생성물 1

HCID 53673871HCID 53673871, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

0.02 mole (5.92 g) of 2,5-dibromo-4-nitroaniline (compound B) is added to 15 ml of 96° ethanol to which 12 ml of ethanolamine have been added. The mixture is heated in refluxing alcohol for 6 h 30 min. After cooling and dilution of the reaction mixture with 100 ml of iced water, the expected product precipitates.

후처리

  1. additionhave been added
  2. temperatureThe mixture is heated
  3. temperatureAfter cooling
  4. customdilution of the reaction mixture with 100 ml of iced water, the expected product precipitates

출처 및 근거

ORD 기록
ord-363bfb4003904efb8b5cf573bf65a281
출처 데이터셋
uspto-grants-1988_02
특허 번호
US04725283

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