Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triphenylphosphine → 2-(4-Bromophenoxy)propyl 2-methylacrylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triphenylphosphine | HCID 11776 | — |
| 반응물 | 2-Hydroxypropyl methacrylate | HCID 13539 | — |
| 반응물 | 2-Bromo-1,4-benzenediol | HCID 68502 | — |
| 반응물 | Diisopropyl azodicarboxylate | HCID 5363146 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 2-(4-Bromophenoxy)propyl 2-methylacrylate | HCID 59005016 | — |
반응 단계
Following the same preparation procedure of Example 2, the reaction was carried out with 4-hydroxy bromophenol (4 g), 2-hydroxypropyl 2-methylacrylate (3.33 g), triphenyl phosphine (6.06 g) and DIAD (4.69 g) in 50 ml of THF to give after chromatography purification pure 2-(4-bromophenoxy)propyl 2-methylacrylate as pale yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08105662B2 |
| 출처 데이터셋 | uspto-grants-2012_01 |
| ORD ID | ord-50bf399bb55646d6837673bbf30e7dea |
| 출처 메모 | uspto-grants-2012_01 |