Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl iodide → Ethyl 6-methoxybenzo[D]isoxazole-3-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Ethyl 6-hydroxybenzo[d]isoxazole-3-carboxylate | HCID 136216618 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Ethyl 6-methoxybenzo[D]isoxazole-3-carboxylate | HCID 53249635 | 19% |
반응 단계
Potassium carbonate (9.42 mmol) and iodomethane (8.45 mmol) were added to a solution of crude ethyl 6-hydroxybenzo[d]isoxazole-3-carboxylate (2.42 mmol) in N,N-dimethylformamide (30 mL) and the reaction mixture was maintained for 48 h at rt in the dark. The reaction mixture was diluted with water (100 mL) and was extracted with ethyl acetate (2×100 mL). The combined organic layers were washed with brine (3×100 mL), dried (magnesium sulfate), and concentrated. The residue was purified by chromatography (30/1 petroleum ether/ethyl acetate) to provide ethyl 6-methoxybenzo[d]isoxazole-3-carboxylate in 19% yield as a yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08106066B2 |
| 출처 데이터셋 | uspto-grants-2012_01 |
| ORD ID | ord-323718e9586a4c898858ef8e34938bb6 |
| 출처 메모 | uspto-grants-2012_01 |