반응식
[CH2:1]=[CH:2][S:3]([O-:6])(=[O:5])=[O:4].[Na+:7].[CH3:8][NH:9][CH3:10]>>[CH3:8][N:9]([CH3:10])[CH2:1][CH2:2][S:3]([O-:6])(=[O:5])=[O:4].[Na+:7]참가 물질
3
실험 절차
Sodium ethylenesulfonate (18.2 ml, 25% aqueous solution w/w) and dimethylamine (4.43 ml, 40% aqueous solution w/w) were heated in a sealed finger tube at 105° C. for 48 h before concentrating in vacuo to yield the subtitle compound as a white solid. Yield: 9.80 g.
후처리
- concentrationbefore concentrating in vacuo
출처 및 근거
- ORD 기록
- ord-3b9b1bfe3c984dff9ebaf9513b9644c9
- 출처 데이터셋
- uspto-grants-2012_01
- 특허 번호
- US08106063B2
연결된 노트
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