Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Piperidine → 1-Piperidinesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Piperidine | HCID 8082 | — |
| 반응물 | Sulfamide | HCID 82267 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | 1-Piperidinesulfonamide | HCID 276741 | — |
반응 단계
Piperidine (3.0 g) and sulfamide (5.93 g) in 1,4-dioxane (100 ml) were heated at reflux for 24 h. The solvent was evaporated under reduced pressure and the resulting solid suspended in CHCl3. The suspension was filtered and the filtrate concentrated in vacuo to afford the subtitle compound as a white solid. Yield: 3.85 g.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08106063B2 |
| 출처 데이터셋 | uspto-grants-2012_01 |
| ORD ID | ord-ee0d5e1762a847a1929db3d27db38938 |
| 출처 메모 | uspto-grants-2012_01 |