Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dibromonaphthalic anhydride → Naphthalic anhydride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dibromonaphthalic anhydride | HCID 87118624 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | Naphthalic anhydride | HCID 6693 | — |
반응 단계
The following morning thin-layer chromatography showed only a trace presence of the dibromonaphthalic anhydride. The reaction mixture was cooled to room temperature followed by the addition of 350 ml of ether. The triethylamine hydrobromide byproduct was removed by filtration. The filtrate was concentrated on the rotary evaporator, to give the diphenylethynyl derivative of the 1,8-naphthalic anhydride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08106142B2 |
| 출처 데이터셋 | uspto-grants-2012_01 |
| ORD ID | ord-a4c31501d93647848a5dd956a975d0b9 |
| 출처 메모 | uspto-grants-2012_01 |