Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nicotinic Acid → 3-Pyridinecarbonyl chloride, hydrochloride (1:1)
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nicotinic Acid | HCID 938 | — |
| 반응물 | Phosphorus oxychloride | HCID 24813 | — |
| 생성물 | 3-Pyridinecarbonyl chloride, hydrochloride (1:1) | HCID 88438 | — |
반응 단계
A solution of nicotinic acid (0.50 g, 4.0 mmol) and POCl3 (5 mL) was heated at reflux for 1.5 h and concentrated. The product obtained was directly used in the next reaction.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08536194B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-d0bbcd6f753245b1a3784a550e794017 |
| 출처 메모 | uspto-grants-2013_09 |