Bromine → 2(4-Bromo-1,3-diphenyl-5-pyrazolyl) amino-2-imidazoline hydrobromide

반응식

[C:1]1([N:7]2[C:11]([NH:12][C:13]3[NH:14][CH2:15][CH2:16][N:17]=3)=[CH:10][C:9]([C:18]3[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=3)=[N:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Br:24]Br>>[BrH:24].[Br:24][C:10]1[C:9]([C:18]2[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=2)=[N:8][N:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[C:11]=1[NH:12][C:13]1[NH:14][CH2:15][CH2:16][N:17]=1

참가 물질

반응물 2

HCID 24408Bromine

HCID 127638562(1,3-Diphenyl-5-pyrazolyl) amino-2-imidazoline

생성물 1

HCID 705949692(4-Bromo-1,3-diphenyl-5-pyrazolyl) amino-2-imidazoline hydrobromide

실험 절차

2(1,3-diphenyl-5-pyrazolyl) amino-2-imidazoline (6.0 g.) was treated with 3.2 g. bromine as described in Example III to give 8.85 g. of the product, mp 273° C., decomposed.

후처리

customto give 8.85 g

출처 및 근거

ORD 기록: ord-e58d263229484e7bae246024ffc770c0
출처 데이터셋: uspto-grants-1979_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04171367

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