Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(2-Bromophenyl)boronic acid → 5-(2-Bromophenyl)-1,3-benzodioxole-4-carbaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (2-Bromophenyl)boronic acid | HCID 2773294 | — |
| 반응물 | 5-Bromo-1,3-benzodioxole-4-carboxaldehyde | HCID 11031640 | — |
| 생성물 | 5-(2-Bromophenyl)-1,3-benzodioxole-4-carbaldehyde | HCID 86658680 | — |
반응 단계
The process described in Method B was followed. 5-Bromo-1,3-benzodioxole-4-carbaldehyde (1.15 g, 5.00 mmol) and 2-bromophenylboronic acid (1.10 g, 5.50 mmol) were used to obtain the title compound. The crude product was purified by column chromatography with a mixture of hexane:ethyl acetate (9:1) as the eluent.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08536210B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-89304411dabb487c91269d35b72d6f0f |
| 출처 메모 | uspto-grants-2013_09 |