Potassium Carbonate → HCID 12698958, 화합물

HRID 426950노트

반응식

HRID 426950 반응식
Cl.[CH:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][C:3]=1[CH:12]([O:19][CH3:20])[CH2:13][N:14]1[CH:18]=[CH:17][N:16]=[CH:15]1.C(=O)([O-])[O-].[K+].[K+]>ClCCl>[CH:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][C:3]=1[CH:12]([O:19][CH3:20])[CH2:13][N:14]1[CH:18]=[CH:17][N:16]=[CH:15]1

참가 물질

4

반응물 2

HCID 11430Potassium CarbonateHCID 126989591-[2-(2-Naphthyl)-2-(methoxy)ethyl]imidazole hydrochloride

생성물 1

HCID 12698958HCID 12698958, 화합물

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

1-[2-(2-naphthyl)-2-(methoxy)ethyl]imidazole hydrochloride (800 mg.) in 50 ml. of dichloromethane is shaken with excess dilute potassium carbonate solution until the salt is completely neutralized. The organic layer is then separated, washed twice with water, dried over magnesium sulfate and evaporated to yield 1-[2-(2-naphthyl)-2-(methoxy)ethyl]-imidazole.

후처리

  1. customThe organic layer is then separated
  2. washwashed twice with water
  3. dry with materialdried over magnesium sulfate
  4. customevaporated

출처 및 근거

ORD 기록
ord-99037d6b6ad94f718cce4b2a707f09d1
출처 데이터셋
uspto-grants-1979_10
특허 번호
US04172141

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