참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | (2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal | HCID 107526 | — |
| 반응물 | aldehydo-D-Xylose | HCID 644160 | — |
| 생성물 | Demannose | HCID 161658 | — |
반응 단계
A mixture of 5.7 g (38.4 mmole) of D-xylose of mp. 153° C. and 6.9 g (38.4 mmole) of D-glucose of mp. 143° C. is heated to approximately 80° C. with 52.7 g (176.8 mmole) of BEPDIB. The readily volatile constituents are then removed in vacuo (10-3Torr). Subsequent distillation gives 7.3 g of bp. 78° C./10-3Torr in addition to 11 g of yellowish residue.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04172195 |
|---|
| 출처 데이터셋 | uspto-grants-1979_10 |
|---|
| ORD ID | ord-a57f12c0dd8146639e6a128631e27211 |
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| 출처 메모 | uspto-grants-1979_10 |
|---|
