Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → 4,4'-Bis(hydroxymethyl)biphenyl
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 4,4'-Bis(acetoxymethyl)biphenyl | HCID 11335507 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 4,4'-Bis(hydroxymethyl)biphenyl | HCID 611786 | 80% |
반응 단계
0.1 moles 4,4'bis(acetoxymethyl)biphenyl (prepared by method C above), 0.4 mole sodium hydroxide as 23 percent aqueous solution and 50 mls ethanol were refluxed for 3 hours with stirring. The reaction mixture was filtered and the precipitate washed with water and dried to yield 0.08 moles product=80 percent of theory. m.p. 195°-97° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04172858 |
| 출처 데이터셋 | uspto-grants-1979_10 |
| ORD ID | ord-e0db6938a15b46bc973c1327f6ad7f43 |
| 출처 메모 | uspto-grants-1979_10 |