1,1-Dimethylhydrazine → 2-(4-Methylvaleryl)furan dimethylhydrazone
반응식
[CH3:1][CH:2]([CH3:12])[CH2:3][CH2:4][C:5]([C:7]1[O:8][CH:9]=[CH:10][CH:11]=1)=O.[CH3:13][N:14]([CH3:16])[NH2:15]>CCO>[CH3:13][N:14]([CH3:16])[N:15]=[C:5]([C:7]1[O:8][CH:9]=[CH:10][CH:11]=1)[CH2:4][CH2:3][CH:2]([CH3:12])[CH3:1]참가 물질
4
실험 절차
A solution of 2-(4-methylvaleryl)furan (1 mmol) and N,N-dimethylhydrazine (1.5 mmol) in EtOH was heated at reflux for 24 h. Evaporation and distilation give 2-(4-methylvaleryl)furan dimethylhydrazone as a brown oil.
후처리
- temperatureat reflux for 24 h
- customEvaporation and distilation
출처 및 근거
- ORD 기록
- ord-96464513d39146bbbbb224707a5a4154
- 출처 데이터셋
- uspto-grants-2001_11
- 특허 번호
- US06312662B1
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