Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4'-Fluoroacetophenone → 1-(4-Acetylphenyl)-4-(4-pyridyl)piperazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4'-Fluoroacetophenone | HCID 9828 | — |
| 반응물 | 4-Fluorobenzophenone | HCID 67663 | — |
| 반응물 | 1-(4-Cinnamoylphenyl)-4-(4-pyridyl)piperazine | HCID 53679170 | — |
| 생성물 | 1-(4-Acetylphenyl)-4-(4-pyridyl)piperazine | HCID 18357135 | 40% |
반응 단계
The 1-(4-acetylphenyl)-4-(4-pyridyl)piperazine used as starting material was prepared as in Example 32, using 4-fluoroacetophenone as starting material in place of 4-fluorobenzophenone to give 1-(4-acetylphenyl)-4-(4-pyridyl)piperazine (40% yield), m.p. 176-177° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06313127B1 |
| 출처 데이터셋 | uspto-grants-2001_11 |
| ORD ID | ord-56cc5e7890734fd8bc4174e1de91c4cf |
| 출처 메모 | uspto-grants-2001_11 |