Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
L-Alanine ethyl ester → N-[(2-phenyl)-2-fluoroacetyl]alanine Ethyl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | L-Alanine ethyl ester | HCID 76507 | — |
| 반응물 | Fluorophenylacetic acid | HCID 102649 | — |
| 생성물 | N-[(2-phenyl)-2-fluoroacetyl]alanine Ethyl Ester | HCID 22894970 | — |
반응 단계
Following General Procedure F above, and using α-fluorophenyl acetic acid (Aldrich) and alanine ethyl ester (Aldrich), the title compound was prepared. The reaction was monitored by tlc on silica gel (Rf=0.75 in 1:1 EtOAc:hexane) and purification was by chromatography on silica gel using 1:2 ethyl acetate/hexanes as the eluent.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06313152B1 |
| 출처 데이터셋 | uspto-grants-2001_11 |
| ORD ID | ord-5ad5394c8ca54bd281cfdbb30f28f725 |
| 출처 메모 | uspto-grants-2001_11 |