1,2,5-Trichloro-3-nitrobenzene → 2,3,5-Trichloroaniline

HRID 429142노트

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HRID 429142 반응식

[Cl:1][C:2]1[C:7]([Cl:8])=[CH:6][C:5]([Cl:9])=[CH:4][C:3]=1[N+:10]([O-])=O>[Fe]>[Cl:1][C:2]1[C:7]([Cl:8])=[CH:6][C:5]([Cl:9])=[CH:4][C:3]=1[NH2:10]

참가 물질

3

반응물 1

HCID 64248491,2,5-Trichloro-3-nitrobenzene

생성물 1

HCID 876762,3,5-Trichloroaniline수율 68%

시약·촉매·용매 1

HCID 23925Iron촉매

실험 절차

2,3,5-Trichloro nitrobenzene (D12) was reduced with iron powder as described in Description 7 to give the title compound (D13) (68%), MH+ 196/198.

출처 및 근거

ORD 기록: ord-221a7bf9f9104774a2cfc1a34cd0c1f4
출처 데이터셋: uspto-grants-2001_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06316450B1

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