Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanimidamide, N,N-diphenyl- → 2-(3-Nitrobenzoyl)-3-phenylaminoacrylonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanimidamide, N,N-diphenyl- | HCID 78296 | — |
| 반응물 | 3-(3-Nitrophenyl)-3-oxopropanenitrile | HCID 12382744 | — |
| 용매 | O-Xylene | HCID 7237 | — |
| 생성물 | 2-(3-Nitrobenzoyl)-3-phenylaminoacrylonitrile | HCID 69686076 | 74% |
반응 단계
A mixture of 2-(3-nitrobenzoyl)acetonitrile (13.75 g, 72.3 mmol) and N,N-diphenylformamidine (14.2 g, 72.3 mmol) in xylene (200 ml) was heated at reflux under nitrogen atmosphere. After 3 h, the reaction mixture was cooled to room temperature and diluted with xylenes to give 2-(3-nitrobenzoyl)-3-phenylaminoacrylonitrile (15.7 g) as a yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06316466B1 |
| 출처 데이터셋 | uspto-grants-2001_11 |
| ORD ID | ord-ce55cb02bb944567852897d7300e51ea |
| 출처 메모 | uspto-grants-2001_11 |