Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methylparaben → Methyl 4-(benzyloxy)benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methylparaben | HCID 7456 | — |
| 반응물 | Sodium hydride | HCID 24758 | — |
| 생성물 | Methyl 4-(benzyloxy)benzoate | HCID 299810 | 175.7% |
반응 단계
The title compound (26.6 g, 110%) was prepared from methyl 4-hydroxybenzoate (15.2 g, 125 mmol) utilising sodium hydride as base, in a similar manner to Intermediate 76. 1H NMR (CDCl3) δ 8.00 (2H, d, J 8.9 Hz), 7.82-7.73 (5H, br m), 6.99 (2H, d, J 8.9 Hz), 5.12 (2H, s) and 3.89 (3H, s). MS (ES) m/e 243 [M+H]+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06319922B1 |
| 출처 데이터셋 | uspto-grants-2001_11 |
| ORD ID | ord-4b2a3c581bfa40f0b22e2037edf4b5ad |
| 출처 메모 | uspto-grants-2001_11 |