Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
tert-Butyl methyl ether → HCID 178435105, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | tert-Butyl methyl ether | HCID 15413 | — |
| 반응물 | 4,5-Dimethylthiazole | HCID 62510 | — |
| 반응물 | 2-Bromo-1-(thiophen-2-yl)ethan-1-one | HCID 2776372 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 178435105 | HCID 178435105 | — |
반응 단계
A solution of 4,5-dimethylthiazole (2,2 g, 19.4 mmol) and 2-bromoacetylthiophene (4 g, 19.4 mmol) in ethyl alcohol (20 mL) was refluxed for 3 hours. It was cooled to room temperature and t-butyl methyl ether (10 mL) was added. The reaction mixture was left at room temperature overnight with stirring. The white product separated and was filtered and dried. It was crystallized from ethyl alcohol (4.42 g, 73%), m.p. 203-205° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06319934B1 |
| 출처 데이터셋 | uspto-grants-2001_11 |
| ORD ID | ord-07544ed515c34ce68a593ce274f675ff |
| 출처 메모 | uspto-grants-2001_11 |