Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pyridine → 9-Anthracenylmethyl-1-piperazinecarboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pyridine | HCID 1049 | — |
| 반응물 | Piperazine | HCID 4837 | — |
| 반응물 | 9-Anthracenemethanol | HCID 73848 | — |
| 반응물 | 4-Nitrophenyl chloroformate | HCID 82129 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 9-Anthracenylmethyl-1-piperazinecarboxylate | HCID 9840073 | — |
반응 단계
PAC is produced by adding 9-anthacenemethanol and pyridine to a solution of p-nitrophenyl chloroformate. Product is isolated to provide a crude anthrylmethyl p-nitrophenyl carbonate, which is then added to a solution of piperazine. The reacted mixture is poured into water and extracted with a solvent, preferably an organic solvent such as toluene. The product is washed and dried to provide 9-anthracenylmethyl-1-piperazinecarboxylate (PAC).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06656737B1 |
| 출처 데이터셋 | uspto-grants-2003_12 |
| ORD ID | ord-93be286c94a04903a525ad5c7e904ac7 |
| 출처 메모 | uspto-grants-2003_12 |