Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dichloromethane methanol → 8-(2-Chloro-5-methoxy-phenyl)-Quinoxaline-5-carboxylic acid (1H-imidazol-2-yl)amide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dichloromethane methanol | HCID 21226129 | — |
| 반응물 | 8-(2-Chloro-5-methoxy-phenyl)-quinoxaline-5-carboxylic acid [3-(4-ethyl-piperazin-1-yl)-phenyl]-amide | HCID 44515980 | — |
| 생성물 | 8-(2-Chloro-5-methoxy-phenyl)-Quinoxaline-5-carboxylic acid (1H-imidazol-2-yl)amide | HCID 44516281 | — |
반응 단계
The title compound was prepared in analogy to the procedures described in Example 14 but using 8-(2-chloro-5-methoxy-phenyl)-quinoxaline-5-carboxylic acid (Example 63) in Step 14.1. Title compound: ESI-MS: 380.0 [M+H]+; tR=3.61 min (System 1); TLC: Rf=0.36 (DCM/MeOH, 95:5).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08536175B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-b7c965b4119b4d0cab780eb52926ea7e |
| 출처 메모 | uspto-grants-2013_09 |