2-Chloroethanol → HCID 18760949, 화합물
반응식
[CH3:1][N:2]1[C:6]([NH:7][CH2:8][CH2:9][CH2:10][N:11]([CH3:13])[CH3:12])=[C:5]([N+:14]([O-:16])=[O:15])[C:4]([CH3:17])=[N:3]1.[Cl:18][CH2:19][CH2:20][OH:21]>C(OCC)(=O)C>[Cl-:18].[CH3:1][N:2]1[C:6]([NH:7][CH2:8][CH2:9][CH2:10][N+:11]([CH2:19][CH2:20][OH:21])([CH3:13])[CH3:12])=[C:5]([N+:14]([O-:16])=[O:15])[C:4]([CH3:17])=[N:3]1참가 물질
4
실험 절차
0.5 g of N-(2,5-dimethyl-4-nitro-2H-pyrazol-3-yl)-N′,N′-dimethylpropane-1,3-diamine and 2.2 g of 2-chloroethanol were introduced into a 10 ml three-necked round-bottomed flask equipped with a magnetic stirrer, a thermometer and a condenser. The reaction medium was maintained at reflux for 2 hours. The medium was cooled to room temperature and diluted with 50 ml of ethyl acetate. The precipitate was filtered off. 0.55 g of [3-(2,5-dimethyl-4-nitro-2H-pyrazol-3-yl-amino)propyl](2-hydroxyethyl)dimethylammonium chloride was obtained in the form of yellow crystals, in a yield of 82%.