Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylformamide → 3-Benzoylbenzoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylformamide | HCID 6228 | — |
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | 3-Benzoylbenzoic acid | HCID 101386 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 3-Benzoylbenzoyl chloride | HCID 12797306 | — |
반응 단계
3-Benzoylbenzoic acid (226 mg, 1.0 mmol) in dichloromethane (1.5 mL) was treated with a solution of oxalyl chloride (1.5 mL of 2 M in dichloromethane, 3 mmol) and a catalytic amount of N,N-dimethylformamide. The reaction was stirred overnight at ambient temperature. The excess oxalyl chloride was removed in vacuo to afford 3-benzoylbenzoyl chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06660753B2 |
| 출처 데이터셋 | uspto-grants-2003_12 |
| ORD ID | ord-89f7efbb78264ad49c49b71e0885df54 |
| 출처 메모 | uspto-grants-2003_12 |