Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methyl-6-nitrophenol → 6-Amino-o-cresol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methyl-6-nitrophenol | HCID 83103 | — |
| 반응물 | 2-Amino-6-chlorophenol | HCID 6486025 | — |
| 생성물 | 6-Amino-o-cresol | HCID 413657 | — |
반응 단계
2-Amino-6-methylphenol was prepared from 2-methyl-6-nitrophenol (0.500 g, 3.26 mmol) in a manner similar to that described for 2-amino-6-chlorophenol. The compound was formed as a black solid (0.030 g, 8%). RP-HPLC (25 to 100% CH3CN in 0.1 N aqueous ammonium acetate over 10 min at 1 mL/min using a Hypersil HS C18, 100 Å, 5 μm, 250×4.6 mm column) tr=5.78 min., 86%; m/z 123 (MH+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06660744B1 |
| 출처 데이터셋 | uspto-grants-2003_12 |
| ORD ID | ord-dba82201038c48639008439e9b2bbb30 |
| 출처 메모 | uspto-grants-2003_12 |