Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tetrahydrothiophene → Methyl-tetrahydrothiophene triflate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tetrahydrothiophene | HCID 1127 | — |
| 반응물 | Methyl triflate | HCID 9526 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Methyl-tetrahydrothiophene triflate | HCID 87659244 | — |
반응 단계
11 mmol of tetrahydrothiophene was dissolved in 10 ml of dichloromethane at 0° C., and about 12 mmol of methyltrifluoromethane sulfonate was slowly dripped to the mixture. As a result, a white solid product in a salt form was obtained after about 5 minutes. The solid product was filtered and dried for 1 hour in an oven at 50° C. to obtain the following product:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08536347B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-9dffcd1064074e23ac42b75b8afab9eb |
| 출처 메모 | uspto-grants-2013_09 |