Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,4-Dichloroaniline → N-(3,4-dichlorophenyl)alanine n-propyl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,4-Dichloroaniline | HCID 7257 | — |
| 반응물 | Propyl pyruvate | HCID 523918 | — |
| 생성물 | N-(3,4-dichlorophenyl)alanine n-propyl Ester | HCID 53940447 | — |
반응 단계
Following General Procedure AA above and using 3,4-dichloroaniline (Aldrich) and n-propyl pyruvate (prepared by following General Procedure AO above using n-propanol in place of iso-butanol), the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel (Rf=0.5 in 25% EtOAc/hexanes) and purification was by preparative plate chromatography (silica gel using 25% EtOAc/hexanes as the eluant).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06667305B1 |
| 출처 데이터셋 | uspto-grants-2003_12 |
| ORD ID | ord-5a99c47586594c45ae55bae05ccd79c5 |
| 출처 메모 | uspto-grants-2003_12 |