Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Naphthylamine → 2-[N-(naphth-2-yl)amino]butanoic Acid Ethyl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Naphthylamine | HCID 7057 | — |
| 반응물 | Butanoic acid, 2-bromo-, ethyl ester | HCID 79039 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | 2-[N-(naphth-2-yl)amino]butanoic Acid Ethyl Ester | HCID 10131322 | — |
반응 단계
Following General Procedure AJ above and using 2-aminonaphthalene (Aldrich) and ethyl 2-bromobutyrate (Aldrich), the title compound was prepared as a solid, m.p. 81-83° C. The reaction was monitored by silica gel tlc (Rf=0.5 in CHCl3). Purification was by chromatography (silica gel using chloroform as the eluant).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06667305B1 |
| 출처 데이터셋 | uspto-grants-2003_12 |
| ORD ID | ord-f3b2d420a4fd4c8b8208c93cae909d68 |
| 출처 메모 | uspto-grants-2003_12 |