Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Boron, trifluoro(methanol)-, (T-4)- → HCID 86584267, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Boron, trifluoro(methanol)-, (T-4)- | HCID 11062313 | — |
| 반응물 | HCID 86584266 | HCID 86584266 | — |
| 생성물 | HCID 86584267 | HCID 86584267 | — |
반응 단계
Into a boron trifluoride methanol complex methanol solution is added ethyl [2-(5-acetylamino-2-chloro-4-fluorophenoxy)phenoxy]acetate, and the mixture is heated while stirring. Thereafter, the reaction solution is concentrated, the residue is dissolved in ethyl acetate, and washed with saturated aqueous sodium bicarbonate, dried over magnesium sulfate, and concentrated to obtain ethyl [2-(5-amino-2-chloro-4-fluorophenoxy)phenoxy]acetate [Intermediate compound A3-23].
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06667413B2 |
| 출처 데이터셋 | uspto-grants-2003_12 |
| ORD ID | ord-33db2df52e6946c8b20f6fd6038ad6ce |
| 출처 메모 | uspto-grants-2003_12 |