Ethylamine → 2,2-Diethoxy-N-ethylethan-1-amine

HRID 434467

반응식

HRID 434467 반응식
[CH2:1]([NH2:3])[CH3:2].Br[CH2:5][CH:6]([O:10][CH2:11][CH3:12])[O:7][CH2:8][CH3:9]>>[CH2:1]([NH:3][CH2:5][CH:6]([O:10][CH2:11][CH3:12])[O:7][CH2:8][CH3:9])[CH3:2]

참가 물질

3

반응물 2

HCID 6341EthylamineHCID 74852Ethane, 2-bromo-1,1-diethoxy-

생성물 1

HCID 125032612,2-Diethoxy-N-ethylethan-1-amine

실험 절차

Ethylamine (38 grams) and 1-bromo-2,2-diethoxyethane (20 grams) were charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture was heated at reflux overnight. After this time the mixture was washed with aqueous sodium hydroxide and the organic phase separated from the aqueous phase. The organic phase was then distilled to yield the desired product N-ethyl-N-(2,2-diethoxyethyl)amine as an oil.

후처리

  1. customequipped with a mechanical stirrer
  2. temperaturethermometer and reflux condenser
  3. temperatureThe reaction mixture was heated
  4. temperatureat reflux overnight
  5. washAfter this time the mixture was washed with aqueous sodium hydroxide
  6. customthe organic phase separated from the aqueous phase
  7. distillationThe organic phase was then distilled

출처 및 근거

ORD 기록
ord-8bfcf25171014b779da7e48d424b7a69
출처 데이터셋
uspto-grants-1983_08
특허 번호
US04397677

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