참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Boric Acid | HCID 7628 | — |
| 반응물 | Gluceptate Sodium | HCID 23664054 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | D-glycero-D-gulo-heptonic acid | HCID 25588 | — |
반응 단계
The diboron ester of glucoheptonic acid was prepared as follows: Approximately 124 grams (2 mols) of boric acid and 248 grams (1 mol) of sodium glucoheptonate were charged to an esterification vessel containing about 600 milliliters of water as a solvent. With stirring, the temperature was maintained at about 25° C. for approximately 30 minutes. The mixture was thereafter diluted to a final volume of one liter with additional water.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04397812 |
|---|
| 출처 데이터셋 | uspto-grants-1983_08 |
|---|
| ORD ID | ord-14aa05a9e70445bf9970977a891a1384 |
|---|
| 출처 메모 | uspto-grants-1983_08 |
|---|
