참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sodium | HCID 5360545 | — |
| 반응물 | Gluceptate Sodium | HCID 23664054 | — |
| 촉매 | Tungstic acid | HCID 1152 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | D-glycero-D-gulo-heptonic acid | HCID 25588 | — |
반응 단계
The tungsten ester of glucoheptonic acid was prepared as follows: Approximately 330 grams (1 mol) of the sodium salt of tungstic acid (sodium tungstate) and 248 grams (1 mol) of sodium glucoheptonate were charged to an esterification vessel containing about 600 ml. of water as a solvent. With stirring, the temperature was maintained at about 25° C. for approximately 30 minutes. The mixture was thereafter diluted to a final volume of one liter with additional water.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04397812 |
|---|
| 출처 데이터셋 | uspto-grants-1983_08 |
|---|
| ORD ID | ord-a6dff78a127d46c4a5007c96bfca2ac7 |
|---|
| 출처 메모 | uspto-grants-1983_08 |
|---|
