Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Aniline → N-phenylcarbamoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Aniline | HCID 6115 | — |
| 반응물 | Phosgene | HCID 6371 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | N-phenylcarbamoyl chloride | HCID 576741 | — |
반응 단계
The intermediate is then reacted with a secondary amine in an aprotic solvent such as toluene at temperatures from room temperature or below up to the boiling point of the solvent. An example of this process is the reaction of phosgene with aniline to yield the intermediate N-(phenyl)carbamyl chloride which is then reacted with N-benzyl-n-butylamine to yield 1-benzyl-1-(n-butyl)-3-(phenyl)urea.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04397868 |
| 출처 데이터셋 | uspto-grants-1983_08 |
| ORD ID | ord-e87810831aea4dcca6a2fde26a49ebcc |
| 출처 메모 | uspto-grants-1983_08 |