Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sulfuric Acid → 5-Methyl-4-(trifluoromethyl)-1H-imidazole-2-carbaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 2-(dimethoxymethyl)-5-methyl-4-(trifluoromethyl)-1H-imidazole | HCID 67549218 | — |
| 생성물 | 5-Methyl-4-(trifluoromethyl)-1H-imidazole-2-carbaldehyde | HCID 86648481 | 7.9% |
반응 단계
The same operation as in Example (33b) was performed using 2-(dimethoxymethyl)-5-methyl-4-(trifluoromethyl)-1H-imidazole obtained in Example (36b) (about 2.17 mmol) and 2 N sulfuric acid (15 mL), to obtain 30.5 mg of the title compound as a white solid (7.9%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08536197B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-498d4b21d8644dc78b259e89ae49cdf6 |
| 출처 메모 | uspto-grants-2013_09 |