Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(dimethoxymethyl)-5-ethyl-4-(trifluoromethyl)-1H-imidazole → 5-Ethyl-4-(trifluoromethyl)-1H-imidazole-2-carbaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(dimethoxymethyl)-5-ethyl-4-(trifluoromethyl)-1H-imidazole | HCID 68406043 | — |
| 용매 | Sulfuric Acid | HCID 1118 | — |
| 생성물 | 5-Ethyl-4-(trifluoromethyl)-1H-imidazole-2-carbaldehyde | HCID 86648487 | 29.1% |
반응 단계
The same operation as in Example (33b) was performed using 2-(dimethoxymethyl)-5-ethyl-4-(trifluoromethyl)-1H-imidazole obtained in Example (39c) (about 4.09 mmol) and 2 N sulfuric acid (30 mL), to obtain 228.3 mg of the title compound as a white solid (29%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08536197B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-c2732bdc31d840f1a6f62f8d8476e4c5 |
| 출처 메모 | uspto-grants-2013_09 |