Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → HCID 20452227, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 1,6-Bis(2,2,6,6-tetramethyl-4-piperidylamino)hexane | HCID 93419 | — |
| 반응물 | HCID 20452243 | HCID 20452243 | — |
| 용매 | O-Xylene | HCID 7237 | — |
| 생성물 | HCID 20452227 | HCID 20452227 | 68.3% |
반응 단계
A stirred mixture of 4,4'(hexamethylenediimino)bis(2,2,6,6-tetramethylpiperidine) (10.0 grams; 0.025 mole), 2-allyloxy-4-chloro-6-t-octylamino-1,3,5-triazine (15.1 grams; 0.05 mole), and powdered sodium hydroxide (2.0 grams; 0.05 mole) in xylene (150 mls) is heated at reflux for 24 hours while removing by-product water by means of a trap. The reaction mixture is filtered while hot to remove insolubles. Upon cooling the filtrate, a white crystalline solid precipitates. The solid is recovered by filtration and dried to obtain 15.7 grams of the desired product, mp 210°-212° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04400505 |
| 출처 데이터셋 | uspto-grants-1983_08 |
| ORD ID | ord-00f27744898545709f42e3e11a37d0a1 |
| 출처 메모 | uspto-grants-1983_08 |