참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Salicylaldehyde | HCID 6998 | — |
| 반응물 | L-Phenylglycine | HCID 99291 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 2-Phenylglycine | HCID 3866 | — |
| 생성물 | 4-Hydroxyphenylglycine | HCID 92143 | — |
반응 단계
6 g of L-phenylglycine or L-p-hydroxyphenylglycine were suspended in a mixture of 20 ml of 95% acetic acid and 0.2 ml (0.05 mole per mole of the L-amino acid used) of salicylaldehyde. The suspension was stirred at 100° C. for 2 hours. After the reaction, the mixture was cooled to room temperature, and the crystalline precipitates were collected by filtration and then washed with methanol. DL-phenylglycine or DL-p-hydroxyphenylglycine was thereby obtained. The results are shown in Table 17.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04401820 |
|---|
| 출처 데이터셋 | uspto-grants-1983_08 |
|---|
| ORD ID | ord-f17dfdb554054d039e49e8fe4c287923 |
|---|
| 출처 메모 | uspto-grants-1983_08 |
|---|
