Thionyl Chloride → HCID 12232349, 화합물
반응식
[F:1][C:2]1[CH:3]=[C:4]([C:7]([S:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[CH:8][CH:9]=1)[CH2:5]O.S(Cl)([Cl:19])=O>C1C=CC=CC=1>[F:1][C:2]1[CH:3]=[C:4]([C:7]([S:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[CH:8][CH:9]=1)[CH2:5][Cl:19]참가 물질
4
실험 절차
129 g of 3-fluoro-6-(phenylthio)-benzyl alcohol are dissolved in 385 ml of benzene and heated under reflux. 73 ml of thionyl chloride are added thereto and the resulting mixture is boiled for a further 30 minutes. The mixture is evaporated under reduced pressure. There is obtained 3-fluoro-6-(phenylthio)-benzyl chloride as a red-brown oil.
후처리
- temperatureheated
- temperatureunder reflux
- customThe mixture is evaporated under reduced pressure
출처 및 근거
- ORD 기록
- ord-a3244294a2e14b69a960741180341767
- 출처 데이터셋
- uspto-grants-1977_02
- 특허 번호
- US04006144
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