Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(Cyclohexylthio)-1H-isoindole-1,3(2H)-dione → Acetylcyclohexyl disulfide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(Cyclohexylthio)-1H-isoindole-1,3(2H)-dione | HCID 28777 | — |
| 반응물 | HCID 178418634 | HCID 178418634 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | Acetylcyclohexyl disulfide | HCID 88807735 | 98% |
반응 단계
Thioacetic acid, 0.044 moles, 3.35 grams, is reacted with N-(cyclohexylthio)phthalimide in 100 ml of benzene and the product recovered following a procedure similar to Example 11. Acetylcyclohexyl disulfide, an amber oil, is recovered in 98% yield (7.5 grams). Analysis gives 51.27%C, 7.41%H and 31.78%S compared to 50.6%C, 7.38%H and 33.7%S calculated for C8H14OS2.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04006155 |
| 출처 데이터셋 | uspto-grants-1977_02 |
| ORD ID | ord-c03ecf6c99684936b0abe146aa4e1bb9 |
| 출처 메모 | uspto-grants-1977_02 |